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  • Initiating Collaboration with Co-ACCESS
  • Beamlines at SSRL
    • Beamline 10-2
  • Equipment at Co-ACCESS
    • HetCat In-Situ Cells
    • Mass Spectrometers & Gas Chromatographs
    • Gas Handling Systems
    • Electrochemistry
    • Co-ACCESS Laboratory
  • XAS Theory/Computation
  • Useful Software
  • Education & Outreach

Co-ACCESS Laboratory

Lab space

Lab space for the users

Co-ACCESS operates a 400 sq foot wet chemistry laboratory specifically designed for catalysis studies. The lab is fully stocked with a diverse array of equipment necessary for the catalysis researcher and is available to collaborators.
For sample preparation

List of Equipment

• 6 ft and 4 ft fume hoods

• Two gas cabinets for flammable and toxic gases

• Argon glove box

• Balances

• Pellet press

• Ovens and furnaces

Glove box with antechambers

glovebox.png

June 28, 2023
Glove box with antechambers at Co-ACCESS lab
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FTIR spectrometer at Co-ACCESS

FTIR.jpg

April 11, 2023
FTIR spectrometer at Co-ACCESS
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Lab space

laboratory.png

April 12, 2023
Lab space
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For sample characterization

Nicolet iS50 FTIR Spectrometer

FTIR spectrometer with external prototyping chamber is available for users.

Find more about FTIR below.

  • FTIR Specifications
  • FTIR Gas Manifolds
  • FTIR Cells
FTIR at Co-ACCESS
Source(s): 
  • Polaris IR (9600-20 cm-1) 

  • NIR/VIS (27000-2000 cm-1)

Beamsplitter(s): 
  • KBr (7800-350 cm-1)

Detector(s): 
  • DLaTGS-KBr [fixed-internal] (12500-350 cm-1)

  • MCT-A [movable-internal/prototyping chamber] (11700-600 cm-1)

FTIR Gas Manifold

FTIR Gas Manifold System

Brooks Smart Interface controlled manifold supporting in-situ FTIR experimentation featuring:

  1. 5 gas feed – standard compressed gases, configurable to specific gas blends

  2. Modulation excitation capable – cycling of two gas streams at frequencies up to ??? hz

  3. Isotope feed – feed inlet + injector loop for isotopes (e.g., 13CO)

  4. Liquid Saturator – allows dosing of vapor feeds

  5. Injector loop – ?? mL loop for controlled dosing of gases to a sample

  6. Reactor bypass module – reactant feed able to bypass reactor for on-line characterization of feed stream via mass spectrometer/GC

DRIFT cell for FTIR
  • Praying Mantis High Temperature Reaction Chamber with Praying Mantis Diffuse Reflection Accessory 


Ed Wolfe Cell for FTIR
  • Insitu Research Transmission FTIR cell


Ribeiro Cell for FTIR
  • FTIR cell developed by the Ribeiro Group at Purdue

Co-ACCESS | Catalysis Science
2575 Sand Hill Road
Menlo Park, CA 94025
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